前言
Chapter 1 General Knowledge of Organic Chemistry Experiments
1.1 Rules for Organic Chemistry Laboratory
1.2 Safety Knowledge in the Organic Laboratory
1.3 Commonly Used Equipment and Apparatus of Organic Chemistry Experiments
1.4 Cleaning and Drying of Glassware
1.5 Heating, Cooling and Drying of Reagents in Organic Chemistry Experiments
1.6 Basic Requirements for Pre-lab Work, Lab Record and Lab Report
Chapter 2 Basic Operations of Organic Chemistry Experiments
Exp.1 Determination of Melting Point
Exp.2 Simple Distillation and Determination of Boiling Point
Exp.3 Recrystallization
Exp.4 Extraction
Exp.5 Vacuum Distillation
Exp.6 Steam Distillation
Exp.7 Fractional Distillation
Exp.8 Column Chromatography
Exp.9 Thin Layer Chromatography
Exp.10 Paper Chromatography
Chapter 3 Preparation Experiments of Organic Compounds
Exp.11 Preparation of Cyclohexene
Exp.12 Preparation of 1-Bromobutane
Exp.13 Preparation of Bromobenzene
Exp.14 Preparation of 2-Methyl-2-Butanol
Exp.15 Preparation of Diphenylmethanol
Exp.16 Preparation of 1, 1'-Binaphthol (a Reference-based Experiment)
Exp.17 Preparation of Di-n-butyl Ether
Exp.18 Preparation of Cyclohexanone
Exp.19 Preparation of Benzalacetone and Dibenzalacetone
Exp.20 Preparation of Benzoin
Exp.21 Preparation of Benzoic Acid
Exp.22 Preparation of Adipic Acid
Exp.23 Preparation of Cinnamic Acid
Exp.24 Preparation of Coumarin-3-carboxylic Acid
Exp.25 Preparation of Furfuryl Alcohol and Furoic Acid
Exp.26 Preparation of Ethyl Acetate
Exp.27 Synthesis of Dibutyl Phthalate
Exp.28 Synthesis of Ethyl Acetoacetate
Exp.29 Preparation of Acetylsalicylic Acid (Aspirin)
Exp.30 Preparation of Acetanilide
Exp.31 Preparation of p-Acetamidobenzenesulfonyl Chloride
Exp.32 Preparation of p-Aminobenzenesulfonamide
Exp.33 Green Synthesis of N-bromosuccinimide
Exp.34 Synthesis of Methyl Orange
Exp.35 The Preparation and Beckmann Rearrangement of Benzophenone Oxime
Exp.36 Preparation of Aniline
Exp.37 Preparation and Resolution of Racemic α-Phenylethylamine
Exp.38 Optical Resolution of Trans-1, 2-diaminocyclohexane
Exp.39 Preparation of 2, 3; 5, 6-Di-O-isopropylidene-α-D-mannofuranose
Exp.40 Isolation of Caffeine from Tea Leaves
Chapter 4 Reactivity Experiments of Organic Compounds
Exp.41 The Preparation and Reactivities of Ethylene and Ethyne
Exp.42 The Reactivities of Aromatic Compounds
Exp.43 The Reactivities of Some Alkyl Halides
Exp.44 The Reactivities of Alcohols and Phenols
Exp.45 The Reactivities of Aldehydes and Ketones
Exp.46 The Reactivities of Carboxylic Acids and Their Derivatives
Exp.47 The Reactivities of Amines
章 有机化学实验的一般知识
1.1 有机化学实验室规则
1.2 有机化学实验室的安全知识
1.3 有机化学实验常用仪器和装置
1.4 玻璃仪器的洗涤和干燥
1.5 有机化学实验中试剂的加热、冷却和干燥
1.6 实验预习、实验记录和实验报告的基本要求
第2章 有机化学实验基本操作
实验1 熔点测定
实验2 简单蒸馏及沸点测定
实验3 重结晶
实验4 萃取
实验5 减压蒸馏
实验6 水蒸气蒸馏
实验7 分馏
实验8 柱色谱
实验9 薄层色谱
实验10 纸色谱
第3章 有机化合物制备实验
实验11 环己烯的制备
实验12 1-溴丁烷的制备
实验13 溴苯的制备
实验14 2-甲基-2-丁醇的制备
实验15 二苯甲醇的制备
实验16 1，1'-联二萘酚的合成（文献实验）
实验17 正丁醚的制备
实验18 环己酮的制备
实验19 苄叉丙酮和二苄叉丙酮的制备
实验20 安息香的制备
实验21 苯甲酸的制备
实验22 己二酸的制备
实验23 肉桂酸的制备
实验24 香豆素-3-羧酸的制备
实验25 呋喃甲醇和呋喃甲酸的制备
实验26 乙酸乙酯的制备
实验27 邻苯二甲酸二丁酯的制备
实验28 乙酰乙酸乙酯的制备
实验29 乙酰水杨酸（阿司匹林）的制备
实验30 乙酰苯胺的制备
实验31 对乙酰氨基苯磺酰氯的制备
实验32 对氨基苯磺酰胺的制备
实验33 N-溴代丁二酰亚胺的绿色合成
实验34 甲基橙的制备
实验35 二苯甲酮肟的制备及贝克曼重排
实验36 苯胺的制备
实验37 外消旋α-苯乙胺的制备和拆分
实验38 反-1，2-二氨基环己烷的手性拆分
实验39 2，3；5，6-二-O-异丙叉基-α-D-呋喃甘露糖的制备
实验40 从茶叶中提取咖啡因
第4章 有机化合物性质实验
实验41 乙烯、乙炔的制备和性质
实验42 芳烃的性质
实验43 卤代烃的性质
实验44 醇和酚的性质
实验45 醛和酮的性质
实验46 羧酸及其衍生物的性质
实验47 胺的性质
参考文献

本书采用英汉两种语言，英文为先，中英文并重。全书分四章，包括：有机化学实验的一般知识；有机化学实验的基本操作；有机化合物的制备；化合物的性质实验。