Chapter 1 Overview
1.1 Introduction
1.2 Characterizing the spatial distribution of adsorbed water in wood
1.2.1 Magnetic resonance imaging technique
1.2.2 Computed tomography scanning technique
1.2.3 Neutron radiography
1.2.4 Vibrational spectroscopic imaging techniques
1.3 Determining molecular interactions between adsorbed water and wood
1.3.1 Near-infrared spectroscopy
1.3.2 Nuclear magnetic resonance technique
1.3.3 Fourier transform infrared spectroscopy
1.3.4 Raman spectroscopy
1.4 Future directions
References
Chapter 2 Quantitative detection of moisture content in heat-treated wood cell walls using miero-FTIR spectroscopy
2.1 Introduction
2.2 Materials and methods
2.2.1 Materials
2.2.2 Micro-FTIR spectrometer
2.2.3 DVS apparatus
2.2.4 Micro-FTIR data processing
2.3 Results and discussion
2.3.1 Qualitatively analyzing moisture sorption
2.3.2 Quantitative analysis of moisture sorption
2.4 Conclusions
References
Chapter 3 Quantitative analysis of moisture sorption in lignin using miero-FTIR spectroscopy
3.1 Introduction
3.2 Materials and methods
3.2.1 Materials
3.2.2 Experimental apparatus for micro-FTIR spectral measurement
3.2.3 Experimental apparatus for moisture content measurement
3.2.4 Micro-FTIR spectral data processing
3.3 Results and discussion
3.3.1 Quantitative analysis of moisture adsorption in lignin
3.3.2 Quantitative evaluation of moisture adsorption in lignin
3.4 Conclusions
References
Chapter 4 Quantitatively characterizing moisture sorption of cellulose using micro-FTIR spectroscopy
4.1 Introduction
4.2 Experiment section
4.2.1 Sample preparation
4.2.2 Micro-FTIR spectroscopy apparatus
4.2.3 DVS apparatus
4.2.4 Spectral data processing
4.3 Results and discussion
4.3.1 Qualitatively analyzing water adsorption of cellulose nanofiber film
4.3.2 Quantitative analysis of water adsorption in cellulose nanofiber film
4.4 Conclusions
References
Chapter 5 Quantitative evaluation of moisture sorption in TEMPO oxidized cellulose using micro-FTIR spectroscopy
5.1 Introduction
5.2 Materials and methods
5.2.1 Materials
5.2.2 Experimental apparatus for micro-FTIR spectroscopy measurement
5.2.3 Determination of moisture content using DVS apparatus
5.2.4 Data processing of micro-FTIR spectra
5.3 Results and discussion
5.3.1 Quantitative analysis of moisture adsorption in TOCNF
5.3.2 Quantitatively evaluating water adsorption of TOCNF
5.4 Conclusions
References
Chapter 6 Molecular association of water with wood cell walls during moisture desorption process examined by micro-FTIR spectroscopy
6.1 Introduction
6.2 Materials and methods
6.2.1 Materials
6.2.2 Experimental instrument for micro-FTIR spectral measurement
6.2.3 Micro-FTIR spectral data processing
6.3 Results and discussion
6.3.1 Effective water sorption sites of wood
6.3.2 Molecular structure change of water during moisture desorption process
6.4 Conclusions
References
Chapter 7 Molecular association of water with heat-treated wood cell walls during moisture adsorption process examined by micro-FTIR spectroscopy
7.1 Introduction
7.2 Experimental section
7.2.1 Sample preparation
7.2.2 Micro-FTIR spectroscopy equipment
7.2.3 Data processing
7.3 Results and discussion
7.3.1 FTIR spectra of the heat-treated wood associated with water molecules
7.3.2 The analysis of difference spectra
7.3.3 Intermolecular interactions between adsorbed water and the heat-treated wood
7.4 Conclusions
References
Chapter 8 Molecular association of adsorbed water with heat-treated wood cell walls during moisture desorption process examined by micro-FTIR spectroscopy
8.1 Introduction