内容推荐 《有机化学实验(双语版)》全书共6章,分别为:有机化学实验的一般知识、有机化学实验的基本操作、有机化学基础性实验、有机化学综合性实验、研究性文献实验和典型实验的学习指导。本书在立足基本能力培养的同时,还补充完善了新型的有机合成技术和综合性实验内容,以实现知识、能力的传承与创新协调发展。结合双语实验教学的特点和存在的问题,本书以英文为主,中文为辅,以期给读者提供一个相对完整的专业英语的学习环境,提升其专业英语的阅读、理解和书写能力。 本书可作为化学、化学工程与工艺、应用化学、能源化学工程、安全工程、材料科学与工程、生物制药、环境科学等专业的双语教学配套实验教材,也可供留学生和相关专业人员参考。 目录 Chapter 1 Introduction of Experimental Organic Chemistry 1.1 The Role of Experimental Organic Chemistry 1.2 General Rules for the Organic Chemistry Experiments 1.3 Safety in the Organic Chemistry Laboratory 1.4 Pre-lab Reports.Notebooks and Lab Reports in the Laboratory 1.5 Common Laboratory Glassware and Equipment 1.6 The Literature of Organic Chemistry 1.7 Green Chemistry in the Organic Laboratory Chapter 2 Basic Operations of Organic Chemistry Experiments 2.1 Heating and Cooling 2.2 Drying Organic Solutions and Solids 2.3 Filtration 2.4 Simple Distillation and Boiling Point 2.5 Fractional Distillation 2.6 Steam Distillation 2.7 Vacuum Distillation 2.8 Extraction and Washing 2.9 Recrystallization 2.10 Sublimation 2.11 Measurement of the Melting Point 2.12 Refluxing 2.13 Stirring Methods 2.14 Water-free and Air-free Operation 2.15 Chromatography Techniques Chapter 3 Fundamental Experiments 3.1 Unsaturated Hydrocarbons Exp.1 Preparation of Cyclohexene Exp.2 Preparation of Phenylacetylene 3.2 Alkyl Halides Exp.3 Preparation of 1-Bromobutane Exp.4 Preparation of 2 Chloro 2 methylbutane 3.3 Alcohols,Phenols and Ethers Exp.5 Preparation of 2-Methyl-2-butanol Exp.6 Preparation of Triphenylmethanol Exp.7 Preparation of Di n-butyl Ether Exp.8 Preparation of Ethyl Phenyl Ether Exp.9 Preparation of o-tert Butylhydroquinone 3.4 Aldehydes and Ketones Exp.10 Preparation of Cyclohexanone Exp.11 Preparation of Acetophenone Exp.12 Preparation of Benzaldehyde 3.5 Carboxylic Acids Exp.13 Preparation of Benzoic Acid Exp.14 Preparation of Cinnamic Acid Exp.15 Preparation of Hexane-1,6 dionic Acid 3.6 Carboxylic Acid Derivatives Exp.16 Preparation of Ethyl Acetate Exp.17 Preparation of nDibutyl Phthalate 3.7 Nitrogen-containing Compounds Exp.18 Preparation of Acetanilide Exp.19 Preparation of Methyl Orange 3.8 Heterocyclic Compounds Exp.20 Preparation of 8-Hydroxyquinoline Exp.21 Extraction and Separation of Caffeine from Tea Leaves Chapter 4 Comprehensive Experiments Exp.1 Preparation of Benzyl Alcohol and Benzoic Acid Exp.2 Preparation of Benzil and Thin-layer Chromatography Exp.3 Preparation of Acetylferrocene and Column Chromatography Exp.4 Preparation of Ethyl Acetoacetate by the Claisen Condensation Reaction Exp.5 Synthesis and Characterization of Aspirin Exp.6 Multi-step Synthesis of Sulfanilamide Exp.7 A Solvent Free Cannizzaro Reaction and Thin-layer Chromatography Exp.8 Preparation of 4-Vinylbenzoic Acid by a Wittig Reaction Exp.9 Preparation of Dimedone via the Robinson Annulation Exp.10 Preparation of Cinnamic Acid by the Knoevenagel Condensation Exp.11 Microwave assisted Preparation of Benzoic Acid and Ethyl Benzoate Chapter 5 Experiments from Research and Literature Exp.1 Synthesis of 3-Substituted Isoindolin-1-ones by Solvent-free Grinding Reaction Exp.2 Electroorganic Synthesis of Nitriles Exp.3 Ultrasonic Assisted Green Protocol for the Synthesis of N,N-bis Phenylsulfamide Exp.4 Clean Synthesis in Water:Uncatalysed Preparation of Ylidenemalononitriles Exp.5 Transition metal-catalyzed Convenient Synthesis of Internal Alkyne Exp.6 N-Heterocyclic Carbene Catalyzed Intramolecular Benzoin Condensation to Access 9,10-Phenanthraquinone Exp.7 Optical Resolution of (★)(S)-Methyl-(S)phenylsulfoximine with (+)-L-Camphorsulfonic Acid Exp.8 Synthesis of Benzyl Acetate in Room Temperature lonic Liquids Exp.9 Green Synthesis of 4-Bromoaniline Exp.10 Pinacol Rearrangement and Photochemical Synthesis of Benzopinacol Chapter 6 Study Guide of Some Typical Experiments Exp.1 Preparation of Cyclohexene (Miniscale Reaction) Exp.2 Preparation of.1 |